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thin film deposition

Enhancing Reactive Sputtering with KDF’s Unique Features

Richard West · April 2, 2024 ·

KDF, with its extensive experience in designing reactive sputtering batch coating production systems, offers several optional features that set it apart from others. These features include:

  • Optimally Designed Gas Rings: KDF’s gas rings are designed to inject the reactive gas into the sputter plasma at the target. This is particularly useful when the reactive gas is nitrogen, an intermediately chemically active gas. The gas ring effectively distributes the reactive gas, utilizing the energy of the sputter plasma to make the reaction more favorable.
  • Pressure Control Package: All KDF systems are equipped with downstream pressure control and highly accurate Mass Flow Controllers (MFCs). This technique maintains a constant rate of reactive gas injection throughout the process, making it the most preferable pressure control technique during reactive sputtering.
  • Prompt Gas Injection: The reactive gas Mass Flow Controllers are located as close as possible to the gas injection port on the chamber. This allows for prompt changes in flow rates with little delay.
  • Power Supplies: KDF utilizes pulsed DC supplies with a wide range of pulse frequency and reverse time for conductive target reactive sputtering. This outpaces the arcing and creates a more stable high deposition rate process. KDF also specializes in reactive RF sputtering with in-house made and system-tuned matching networks.

 

KDF Reactive Sputtering System

KDF has extensive experience designing reactive sputtering batch coating production systems. What sets KDF apart are the several optional features that can be added to our reactive sputtering systems.

  • Gas Rings
    • KDF has optimally designed gas rings to inject the reactive gas into the sputter plasma at the target. This is extremely useful, especially when the reactive gas is nitrogen. Since diatomic nitrogen is considered an intermediately chemically active gas, it is best to cycle it through a plasma to crack it into monoatomic form. Essentially, the gas ring effectively distributes the reactive gas to utilize the energy of the sputter plasma to make the reaction more favorable.
  • Pressure Control Package
    • KDF systems are all equipped with downstream pressure control and highly accurate Mass Flow Controllers (MFCs). Downstream pressure control is where the high vacuum gate valve will automatically adjust its position to maintain deposition pressure, and the MFCs can be held at a constant flow rate. This is the most preferable pressure control technique during reactive sputtering, as a constant rate of reactive gas is injected throughout the process.
  • Gas Injection
    • The reactive gas Mass Flow Controllers are properly located to be as close as possible to the gas injection port on the chamber. This allows for the flow rates to be promptly changed with little delay.
  • Power Supplies
    • If using a conductive target to reactively sputter, KDF utilizes pulsed DC supplies with a wide range of pulse frequency and reverse time. This gives more capability to outpace the arcing and creates a more stable high deposition rate process. KDF also specializes in reactive RF sputtering with matching networks made in-house and tuned to each system.
      • High rate processes for deposition of dielectric films have been developed using Pulsed DC reactive sputtering on scanning batch tools. A typical high rate process for the deposition of silicon dioxide films from a conductively doped silicon target would allow the formation of nearly one micron of SiO2 in fifteen minutes, as compared with nearly five hours when RF magnetron sputtered from a quartz target.
        (Ref: Photonics Spectra, pp. 30-31, November 2002)
  • Sputter Sources
    • KDF has specially designed and patented sputter sources that are a great match for a reactive sputtering process. The LMM sputter source, for example, has nearly full-face erosion of the sputter target greatly reducing the build-up of reacted species on the target surface. Also, the inset sputter sources only have target material where the sputter plasma creates an erosion groove for high target utilization and limited area to build up reactive species on the target surface. By reducing the varied amount of reaction on a target surface decreases the chances of potential differences building up causing dreaded arcing and process instability.
  • In-situ Monitoring
    • KDF effectively integrates Plasma Emission Monitoring (PEM) into the system with precisely placed optical sensors and easy-to-use software controls. The PEM tracks the relative emission intensity of the ionized species in the sputtering plasma and controls the reactive gas to maintain an emission intensity setpoint. This emission setpoint correlates to the deposition rate and reactive gas concentration in the films. It is a great solution for rapidly developing a reactive sputtering process and repeatably depositing films of similar quality.

Explanation of Various Sputtering Modes

Vishal Agrawal · July 23, 2021 ·

Written by Ammar Derraa

04/30/2021

Thin film sputtering, including metal, dielectric, and reactive sputtering can be achieved in one of the following modes: DC sputtering, RF sputtering, Pulsed DC sputtering, and HIPIMS sputtering.

Early mode of sputtering was DC (Direct Current), and represented the simplest and most practical method of metal film deposition. As the demand for thin films application has been growing, sputtering technology has been constantly refined and improved to meet the industry challenges. Today’s sputtering involves many configurations such as, DC magnetron, RF (radio frequency), Pulsed DC, and the newly HIPIMS sputtering. DC magnetron is an enhancement for DC sputtering and does improve the deposition rate. RF sputtering expands the use of sputtering to non-metals. Pulsed DC is another enhancement for DC magnetron mode to optimize reactive processes. The recently-developed HIPIMS sputtering has the advantage of yielding hard coating and enhance step coverage in high-aspect applications.

DC Magnetron Sputtering

The DC sputtering mode in a diode configuration is slow and temperature limited. Magnetically Enhanced Sputtering utilizes a magnetic field that is at right angles to the electric field to increase ionization efficiency in the plasma and confine the electrons near the target. Thus, enhancing the deposition rate without overheat. In fact, Magnetron sputtering offers sputtering rates that are an order of magnitude higher than conventional DC method. This is achieved by a set of magnets mounted on the back of the target.

RF Sputtering

RF sputtering is similar to DC sputtering, but uses an applied RF voltage to eliminate charge buildup on the target. RF sputtering can operate in a diode or magnetron-enhanced configuration. The advantage of reactive sputtering is the ability to sputter dielectric target like quartz.

Pulsed DC Sputtering

Pulsed DC sputtering is used to minimize arcing and target poising in reactive processes. This is achieved by pulsing the applied voltage with a frequency in the range of 1-360kHz. The voltage is reversed for about 1 micron-second to clean any reactive buildup on the target.

Reactive Sputtering

Reactive sputtering refers to the sputtering of a chemically reactive target material in the presence of a reactive gas (usually oxygen or nitrogen) in order to deposit a nitride or an oxide compound film. Since the reactive process can occur in both DC and RF sputtering, either mode can be used for reactive sputtering.  In DC reactive sputtering, chemical reactions do take place on the target surface forming an insulating layer on the target surface. However, in RF sputtering the insulating layer is sputtered away as soon as it forms. Pulsed DC sputtering minimizes this this target poising issue.

HIPIMS Sputtering

HIPIMS (High Power Impulse Magnetron Sputtering) is a new sputtering technique that can produce highly dense, smooth, and hard films with enhanced conformity or step-coverage for high aspect ratio applications. This is the result of a highly dense and ionized plasma that is generated by HIPIMS. In conventional magnetron sputtering, increasing plasma density through power is limited by heat dissipation for any practical gain, and the production of ionized plasma is not a simple task. HIPIMS is based on the use of special power supplies with of a very high voltage to generate short pulses of energy up to a Megawatt peak power. Thus, creating a very highly dense and ionized plasma. KDF has an extensive experience with HIPIMS, and has already developed and optimized many HIPIMS deposition processes along software integration, some of which are currently being used in a manufacturing environment.

Solutions in Action

Rad Horak · February 25, 2017 ·

Today’s consumers are accustomed to a certain level of imperfection in electronic devices.

An LED flashlight may fail. A laptop may no longer boot up the way it did just yesterday. But while these everyday equipment deficiencies may be accepted as part of modern living, the stakes are much higher when it comes to medical devices.

“Our customers in the implantable medical device industry demand the highest level of quality and precision,” said Todd Plaisted, director of marketing, KDF. “Equipment failure to perform is simply not an option for companies that produce pacemakers and defibrillators.”

844i Series systems
Like all KDF sputtering tools, 844i Series systems are designed to meet demanding processing
requirements and feature an intuitive interface to monitor parameters.

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Founded in 1986, KDF is a leading supplier of physical vapor deposition (PVD) batch inline sputtering tools. These vacuum coating systems are used in the production of mainstream silicon, emerging materials, fl at panel displays, optical communications and medical devices. From headquarters in Rockleigh, New Jersey, KDF serves a global customer base and supports more than 3,300 systems in the field.

“More than half of the semiconductor fabs in the world use a KDF system in wafer processing,” Plaisted said. “And we extend the same quality the medical device market demands to all industries we serve.”

Virtually always located in a cleanroom environment, sputtering tools precisely deposit thin films of various materials, metals and/or dielectrics onto a substrate.

Next, the wafers typically enter etching or patterning equipment. Depending on the application, the substrate can return to the sputtering system several times during the manufacturing process to add different layers.

“Recipe management is critical throughout this process,” said Marc Fregeau, software development manager, KDF. “We develop all the programming for our customers – and update the software for them as their processes change.”

As more companies embrace contract fabrication, recipe control and monitoring has become increasingly important. In this emerging business model, a manufacturer provides fabrication services for a wide range of customers – each requiring different processes.

In 2010, KDF adopted a Rockwell Automation® control and information platform for their equipment featuring an Allen-Bradley® CompactLogix™ controller and an RSView®32 HMI solution.

“The initial control solution met our requirements,” Fregeau explained. “But as our customers’ process requirements became more demanding, we needed a more robust visualization solution that could grow with us.”

To enhance system performance, the company recently migrated to a FactoryTalk® View Site Edition (SE) HMI platform. In addition, the company opted for a CompactLogix 5370 controller (L36ERM), which features faster processor speeds and supports up to 16 axes of integrated motion over an EtherNet/IP™ network.

“Moving from the 32-bit HMI to the 64-bit FactoryTalk View solution was key,” Fregeau explained. “It provides a framework for an easy-to-use recipe management system – and the capacity to meet the demand for real-time information in a complex process environment.”

KDF systems are designed to monitor all process parameters including power supply voltages, sputter gas pressures/ratios, residual gas analyzer (RGA) background species vacuum integrity checks, substrate temperatures and more. The FactoryTalk View application helps enable real-time operator monitoring of those parameters through intuitive displays – and provides an audit trail of operator and alarm information in a centralized log database for absolute process validation.

“If there’s a process anomaly, the data logging helps determine the root cause,” Fregeau said. “The system also allows us to actively take ‘snapshots’ of the process in real time for reporting purposes.”

As an option, KDF customers can add FactoryTalk Historian to their system. FactoryTalk Historian features built-in connectivity to FactoryTalk View and provides robust, high-speed data collection and analysis capabilities.

For efficient system development, KDF applies the same Rockwell Automation control and visualization platform across its complete machine portfolio.

“Our sputtering tools share many components – as well as the control system,” Plaisted said. “A shared platform allows us to develop versatile equipment very cost-effectively.”

Looking toward the future, KDF is positioned to respond to fluctuating customer requirements – and an unpredictable marketplace.

“We are constantly changing,” Plaisted said. “And the Rockwell Automation control environment allows us to configure our tools and make changes as we need them.”

View the original article

TFR Technologies Selects KDF 954NTX with ERPP Option for Uniform, Repeatable Thin Film Deposition

Rad Horak · September 24, 2015 ·

KDF RELEASE 2004

KDF today announced that TFR Technologies, Inc. has placed an order for a KDF 954NTX in-line sputtering system with an enhanced rotating planetary pallet (ERPP) option. This is the first order of a KDF system ever placed by TFR Technologies.

TFR selected the KDF tool after an extensive evaluation of physical vapor deposition (PVD) solutions, which concluded that the KDF 954NTX with an ERPP option provided the best combination of performance, yield and throughput to suit the company’s needs for miniature high performance frequency control device manufacturing.

“KDF is very pleased to announce that TFR Technologies has joined our global customer base,” said Kurt Flechsig, KDF president. “By choosing the KDF 954NTX, TFR Technologies validates the superiority of our technology for uniform, stable deposition of thin films in resonator manufacturing.”

The expansion of thin film device capabilities is driving the need for better uniformity and higher repeatability for thin film deposition. Using KDF’s proprietary ERPP in conjunction with the standard linear scanning mode on the KDF 954NTX provides excellent uniformity and repeatability, enabling the production of complex multi-layer dielectric coats such as mirrors and filters in a highly repeatable and uniform manner.

“TFR is looking forward to the KDF sputtering unit enabling higher volume production by increasing throughput across a wide range of depositions,” said Shane Leiphart, Senior Process Engineer, TFR Technologies, Inc. “It is expected that this tool will meet the company’s requirement for overall thin film performance well into the future.”

The 954NTX is a four-target in-line sputtering tool for front- and backside deposition. The tool, which is optimized for compound semiconductor processing applications, features a low cost of ownership, and enables high utilization and throughput. Like all KDF 900 Series tools, the 954NTX offers users the capability of a production tool with the process flexibility typically found in an R&D system. The 900 Series exceeds requirements for deposition of thin films in application critical devices and other applications requiring the absolute in uniformity.

The KDF 954NTX is one of KDF’s popular X Series™ products. It features the latest KDF cathode designs, which have been lengthened to 17 inches, offering improved uniformity over the entire pallet. X Series cathodes are also available in both Planar and Inset™ cathode form.

# # #
About KDF
KDF Electronic & Vacuum Services, Inc., produces batch in-line sputtering tools in a wide variety of R&D and production formats for the mainstream silicon, emerging materials and flat-panel display markets. KDF systems are used in the production of semiconductors, photomasks, telecommunications networks, wireless circuits, gallium arsenide (GaAs), high density interconnect, sensors, optoelectronics, flat panel display and radio frequency power devices. KDF is located in Rockleigh, New Jersey, and has representatives in Europe, Japan, Taiwan, Singapore, Malaysia, China and Korea.
Company Contacts
Kurt Flechsig
President & CEO
Tel: +1 (201) 784-5005
E-mail: kurt@kdf.com

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We offer the most advanced and reliable physical vapor deposition batch in-line sputtering tools at the industry’s lowest cost of ownership. KDF systems can be customized to meet the customer’s needs and cover a wide variety of process requirements for the mainstream silicon, emerging materials and flat panel display markets.

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